2002
Precursor Morphology Controlled Formation of Rutile VO2 Nanorods and Their Self-Assembled Structure
Gui Z, Fan R, Mo W, Chen X, Yang L, Zhang S, Hu Y, Wang Z, Fan W. Precursor Morphology Controlled Formation of Rutile VO2 Nanorods and Their Self-Assembled Structure. Chemistry Of Materials 2002, 14: 5053-5056. DOI: 10.1021/cm020178f.Peer-Reviewed Original ResearchVO2 nanorodsPrecursor morphologyX-ray energy-dispersive spectroscopy techniquesSelf-assembled structuresX-ray powder diffractionElectron microscopyOne-dimensional morphologyEnergy dispersive spectroscopy (EDS) techniquesDifferential scanning calorimetryArea electron diffractionHydrothermal reactionTransmission electron microscopyThermogravimetric analysisReaction detailsSealed autoclavePowder diffractionSpectroscopy techniquesScanning calorimetryNanorodsNanocrystalline domainsHigh-resolution electron microscopyElectron diffractionDiffractionMorphologyLow temperature
2001
A New Metastable Phase of Needle-like Nanocrystalline VO2·H2O and Phase Transformation
Gui Z, Fan R, Chen X, Wu Y. A New Metastable Phase of Needle-like Nanocrystalline VO2·H2O and Phase Transformation. Journal Of Solid State Chemistry 2001, 157: 250-254. DOI: 10.1006/jssc.2000.9037.Peer-Reviewed Original ResearchArea electron diffractionTransmission electron microscopyNew metastable phaseX-ray powder diffractionChemical reaction conditionsElectron microscopyElectron diffractionN2H4 concentrationHydrothermal reactionPowder diffractionMetastable phaseThermogravimetric analysisPhase transformationOptimum conditionsDiffractionReaction conditionsNanocrystallitesFinal productDifferential scanning calorimetryMicroscopyNH4VO3Scanning calorimetrySpectroscopyHydrazineLow-Temperature Hydrothermal Synthesis of Transition Metal Dichalcogenides
Chen, Fan R. Low-Temperature Hydrothermal Synthesis of Transition Metal Dichalcogenides. Chemistry Of Materials 2001, 13: 802-805. DOI: 10.1021/cm000517+.Peer-Reviewed Original ResearchTransition metal dichalcogenidesTransition metal saltsMetal dichalcogenidesTemperature hydrothermal synthesisDifferent reaction conditionsNew aqueous solutionPyrite NiS2Transmission electron microscopy imagesMetal saltsHydrothermal synthesisHydrothermal reactionAqueous solutionReaction conditionsElectron microscopy imagesNature of productsSurface areaMicroscopy imagesDichalcogenidesLow temperatureNa2SeSO3NiSe2NiS2FeS2CoS2SynthesisA new simple hydrothermal preparation of nanocrystalline magnetite Fe3O4
Fan R, Chen X, Gui Z, Liu L, Chen Z. A new simple hydrothermal preparation of nanocrystalline magnetite Fe3O4. Materials Research Bulletin 2001, 36: 497-502. DOI: 10.1016/s0025-5408(01)00527-x.Peer-Reviewed Original ResearchX-ray photoelectron spectroscopyInverse cubic spinel structureMagnetite particlesTraditional chemical analysisSimple hydrothermal preparationCubic spinel structureTransmission electron microscopy imagesX-ray powder diffraction patternsPhotoelectron spectroscopySingle-phase magnetiteHydrothermal reactionHydrothermal preparationElectron microscopy imagesSpinel structurePowder diffraction patternsChemical analysisSodium hydroxideAverage diameterMagnetite Fe3O4Sodium thiosulfateDiffraction patternsMicroscopy imagesFerrous sulfateSpectroscopyFe3O4
2000
A Novel Route to Obtain Molybdenum Dichalcogenides by Hydrothermal Reaction
Fan R, Chen X, Chen Z. A Novel Route to Obtain Molybdenum Dichalcogenides by Hydrothermal Reaction. Chemistry Letters 2000, 29: 920-921. DOI: 10.1246/cl.2000.920.Peer-Reviewed Original ResearchHydrothermal reactionX-ray photoelectron spectroscopyX-ray powder diffractionTransmission electron microscopy imagesAverage particle sizePhotoelectron spectroscopyHydrazine monohydrateSamples of MoS2Electron microscopy imagesMolybdenum dichalcogenidesGood yieldsPowder diffractionNovel routeChemical analysisNano-crystallitesParticle sizeMicroscopy imagesMoS2ReactionSpectroscopyNa2MoO4DiffractionMonohydrateDichalcogenidesMoSe2